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对硝基乙酰苯胺

对硝基乙酰苯胺用途

【用途一】
用作药物和染料的中间体。

对硝基乙酰苯胺名称

[ CAS 号 ]:
104-04-1

[ 中文名 ]:
对硝基乙酰苯胺

[ 英文名 ]:
4-Nitroacetanilide

[中文别名 ]:

[英文别名 ]:

Acetanilide, p-nitro-
N1-(4-nitrophenyl)acetamide
N-Acetyl-p-nitroaniline
4‘-Nitroacetanilide
Acetanilide,p-nitro
acetic acid p-nitroanilide
EINECS 203-169-0
Acetanilide,4'-nitro
4′-Nitroacetanilide
4-NITROACETANILIDE

对硝基乙酰苯胺物理化学性质

[ 密度 ]:
1.3±0.1 g/cm3

[ 沸点 ]:
408.9±28.0 °C at 760 mmHg

[ 熔点 ]:
213-215 °C(lit.)

[ 分子式 ]:
C₈H₈N₂O₃

[ 分子量 ]:
180.161

[ 闪点 ]:
201.1±24.0 °C

[ 精确质量 ]:
180.053497

[ PSA ]:
74.92000

[ LogP ]:
1.66

[ 外观性状 ]:
黄色至绿色-棕色结晶粉末

[ 蒸汽压 ]:
0.0±1.0 mmHg at 25°C

[ 折射率 ]:
1.618

[ 储存条件 ]:
2-8°C

[ 稳定性 ]:
Stable. Combustible. Incompatible with strong oxidizing agents.

对硝基乙酰苯胺MSDS

对硝基乙酰苯胺毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: AE5075000

CHEMICAL NAME :: Acetanilide, p-nitro-

CAS REGISTRY NUMBER :: 104-04-1

LAST UPDATED :: 199701

DATA ITEMS CITED :: 2

MOLECULAR FORMULA :: C8-H8-N2-O3

MOLECULAR WEIGHT :: 180.18

WISWESSER LINE NOTATION :: WNR DMV1

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LDLo - Lowest published lethal dose

ROUTE OF EXPOSURE :: Intraperitoneal

SPECIES OBSERVED :: Rodent - rat

DOSE/DURATION :: 500 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: NCNSA6 National Academy of Sciences, National Research Council, Chemical-Biological Coordination Center, Review. (Washington, DC) Volume(issue)/page/year: 5,10,1953

对硝基乙酰苯胺安全信息

[ 符号 ]:

GHS07

[ 信号词 ]:
Warning

[ 危害声明 ]:
H315-H319-H335

[ 警示性声明 ]:
P261-P305 + P351 + P338

[ 个人防护装备 ]:
dust mask type N95 (US);Eyeshields;Gloves

[ 危害码 (欧洲) ]:
Xi

[ 风险声明 (欧洲) ]:
R36/37/38

[ 安全声明 (欧洲) ]:
S26-S36

[ 危险品运输编码 ]:
NONH for all modes of transport

[ WGK德国 ]:
3

[ RTECS号 ]:
AE5075000

[ 海关编码 ]:
2924299090

对硝基乙酰苯胺合成路线

对硝基乙酰苯胺上下游产品

对硝基乙酰苯胺上游产品

对硝基乙酰苯胺下游产品

对硝基乙酰苯胺制备

由乙酰苯胺经硝化制得。将98%的硫酸675kg加入硝化锅内，搅拌，并在20-25℃，2-2.5h内加入99%的乙酰苯胺225kg。待全部溶解后，降温至7℃，在4-7℃约20h内滴加混酸（由63kg水、60kg98%硫酸及107kg96%硝酸配成）。滴加完毕，稀释于4000L冰水中，静置1h。虹吸分离上层废酸，将下层物料过滤，用水洗至中性，即得4-硝基乙酰苯胺。另一种制法是用对硝基苯胺经乙酰化而得。

对硝基乙酰苯胺海关

[ 海关编码 ]: 2924299090

[ 中文概述 ]:
2924299090. 其他环酰胺（包括环氨基甲酸酯）（包括其衍生物以及他们的盐）. 增值税率:17.0%. 退税率:13.0%. 监管条件:无. 最惠国关税:6.5%. 普通关税:30.0%

[ 申报要素 ]: 品名, 成分含量, 用途, 包装

[ Summary ]:
2924299090. other cyclic amides (including cyclic carbamates) and their derivatives; salts thereof. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:30.0%

对硝基乙酰苯胺文献

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The use of high-temperature conversion (HTC) reduction systems interfaced with isotope ratio mass spectrometers for δ(18)O measurements of nitrogen-containing organic materials is complicated by isoba...

Dinuclear Nickel(II) Complexes as Models for the Active Site of Urease.

Inorg. Chem. 35(13) , 3792-3803, (1996)

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Gene cloning and characterization of arylamineN-acetyltransferase fromBacillus cereusstrain 10-L-2

J. Biosci. Bioeng. 107(1) , 27-32, (2009)

Bacillus cereus strain 10-L-2 synthesizes two arylamine N-acetyltransferases (Nat-a and Nat-b) with broad substrate specificities toward aniline and its derivatives. In southern blot analysis using pr...

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