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2-硝基苯乙酮

2-硝基苯乙酮用途

用作感光材料的中间体.可用作医药中间体

2-硝基苯乙酮名称

[ CAS 号 ]:
577-59-3

[ 中文名 ]:
邻硝基苯乙酮

[ 英文名 ]:
2′-Nitroacetophenone

[中文别名 ]:

[英文别名 ]:

1-(2-Nitrophenyl)ethan-1-one
2-Nitroacetophene
O-NITROACETOPHENONE
1-(2-Nitrophenyl)ethanone
o-Acetylnitrobenzene
2-Acetylnitrobenzene
2`-Nitroacetophenone
MFCD00007259
1-(2-Nitrophenyl)-1-ethanone
WNR BV1

2-硝基苯乙酮物理化学性质

[ 密度 ]:
1.23

[ 沸点 ]:
286.4±13.0 °C at 760 mmHg

[ 熔点 ]:
76-78 °C(lit.)

[ 分子式 ]:
C₈H₇NO₃

[ 分子量 ]:
165.146

[ 闪点 ]:
137.8±12.6 °C

[ 精确质量 ]:
165.042587

[ PSA ]:
62.89000

[ LogP ]:
1.28

[ 外观性状 ]:
黄色-绿色液体或晶体

[ 蒸汽压 ]:
0.0±0.6 mmHg at 25°C

[ 折射率 ]:
1.558

[ 储存条件 ]:
Refrigerator

[ 稳定性 ]:
Stable. Combustible. Incompatible with strong oxidizing agents.

[ 水溶解性 ]:
Insoluble

2-硝基苯乙酮MSDS

2-硝基苯乙酮毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: AM9600000

CHEMICAL NAME :: Acetophenone, 2'-nitro-

CAS REGISTRY NUMBER :: 577-59-3

BEILSTEIN REFERENCE NO. :: 1102322

LAST UPDATED :: 199709

DATA ITEMS CITED :: 5

MOLECULAR FORMULA :: C8-H7-N-O3

MOLECULAR WEIGHT :: 165.16

WISWESSER LINE NOTATION :: WNR BV1

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Oral

SPECIES OBSERVED :: Rodent - rat

DOSE/DURATION :: 1600 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Oral

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 800 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Administration onto the skin

SPECIES OBSERVED :: Mammal - species unspecified

DOSE/DURATION :: >20 gm/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

MUTATION DATA

TYPE OF TEST :: DNA repair

TEST SYSTEM :: Bacteria - Bacillus subtilis

DOSE/DURATION :: 5 uL/disc

REFERENCE :: MUREAV Mutation Research. (Elsevier Science Pub. B.V., POB 211, 1000 AE Amsterdam, Netherlands) V.1- 1964- Volume(issue)/page/year: 170,11,1986

2-硝基苯乙酮安全信息

[ 符号 ]:

GHS07

[ 信号词 ]:
Warning

[ 危害声明 ]:
H302

[ 个人防护装备 ]:
Eyeshields;Faceshields;full-face respirator (US);Gloves;multi-purpose combination respirator cartridge (US);type ABEK (EN14387) respirator filter

[ 危害码 (欧洲) ]:
Xn:Harmful;

[ 风险声明 (欧洲) ]:
R22

[ 安全声明 (欧洲) ]:
S22-S24/25

[ 危险品运输编码 ]:
NONH for all modes of transport

[ WGK德国 ]:
3

[ RTECS号 ]:
AM9625000

[ 包装等级 ]:
III

[ 危险类别 ]:
6.1

[ 海关编码 ]:
29147090

2-硝基苯乙酮合成路线

2-硝基苯乙酮上下游产品

2-硝基苯乙酮上游产品

2-硝基苯乙酮下游产品

2-硝基苯乙酮制备

制备方法：由邻硝基乙苯经氧化而得。将邻硝基乙苯、癸酸以及引发剂偶氮二异丁腈加入反应塔，同时将空气缓缓通入塔内，保持压力0.3-0.8MPa，控制在120-130℃下氧化生成2-硝基苯乙酮。

2-硝基苯乙酮海关

[ 海关编码 ]: 2914700090

[ 中文概述 ]:
2914700090 其他酮及醌的卤化、磺化衍生物（包括硝化和亚硝化衍生物）. 增值税率:17.0% 退税率:9.0% 监管条件:无最惠国关税:5.5% 普通关税:30.0%

[ 申报要素 ]: 品名, 成分含量, 用途, 丙酮报明包装

[ Summary ]:
HS: 2914700090 halogenated, sulphonated, nitrated or nitrosated derivatives of ketones and quinones, whether or not with other oxygen function Tax rebate rate:9.0% Supervision conditions:none VAT:17.0% MFN tariff:5.5% General tariff:30.0%