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4-Aminodiphenylamine

Names

[ CAS No. ]:
101-54-2

[ Name ]:
4-Aminodiphenylamine

[Synonym ]:
azoic diazo no. 22
1,2-Benzenediamine, N-phenyl-
ZR DMR
p-Aminodiphenylamine
N-phenyl-1,2-phenylenediamine
Variamine Blue RT
N1-Phenylbenzene-1,4-diamine
N-Phenyl-p-Phenylenediamine
N-Phenyl-1,4-phenylenediamine
Variamine Blue RT Salt
N-Phenyl-1,2-benzenediamine
n-phenyl-o-phenylenediamine
N-Phenyl-1,4-benzenediamine
4-Aminodiphenylamine
Azoic Diazo Component 22
4-N-phenylbenzene-1,4-diamine
o-semidine
MFCD00007850
1,4-Benzenediamine, N-phenyl-
N-PHENYLBENZENE-1,2-DIAMINE
EINECS 202-951-9

Chemical & Physical Properties

[ Density]:
1.2±0.1 g/cm3

[ Boiling Point ]:
354.7±15.0 °C at 760 mmHg

[ Melting Point ]:
69 °C

[ Molecular Formula ]:
C12H12N2

[ Molecular Weight ]:
184.237

[ Flash Point ]:
197.8±24.0 °C

[ Exact Mass ]:
184.100052

[ PSA ]:
38.05000

[ LogP ]:
1.29

[ Vapour Pressure ]:
0.0±0.8 mmHg at 25°C

[ Index of Refraction ]:
1.684

MSDS

Toxicological Information

CHEMICAL IDENTIFICATION

RTECS NUMBER :
ST3150000
CHEMICAL NAME :
p-Phenylenediamine, N-phenyl-
CAS REGISTRY NUMBER :
101-54-2
LAST UPDATED :
199710
DATA ITEMS CITED :
15
MOLECULAR FORMULA :
C12-H12-N2
MOLECULAR WEIGHT :
184.26
WISWESSER LINE NOTATION :
ZR DMR

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :
Standard Draize test
ROUTE OF EXPOSURE :
Administration into the eye
SPECIES OBSERVED :
Rodent - rabbit
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
464 mg/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - mouse
DOSE/DURATION :
244 mg/kg
TOXIC EFFECTS :
Blood - hemorrhage Nutritional and Gross Metabolic - body temperature decrease
TYPE OF TEST :
LDLo - Lowest published lethal dose
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Mammal - cat
DOSE/DURATION :
100 mg/kg
TOXIC EFFECTS :
Lungs, Thorax, or Respiration - cyanosis Blood - methemoglobinemia-carboxyhemoglobin
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rabbit
DOSE/DURATION :
>5 gm/kg
TOXIC EFFECTS :
Details of toxic effects not reported other than lethal dose value
TYPE OF TEST :
LD50 - Lethal dose, 50 percent kill
ROUTE OF EXPOSURE :
Administration onto the skin
SPECIES OBSERVED :
Rodent - rabbit
DOSE/DURATION :
>5 gm/kg
TOXIC EFFECTS :
Sense Organs and Special Senses (Olfaction) - effect, not otherwise specified Sense Organs and Special Senses (Eye) - effect, not otherwise specified Behavioral - food intake (animal)
TYPE OF TEST :
TDLo - Lowest published toxic dose
ROUTE OF EXPOSURE :
Oral
SPECIES OBSERVED :
Rodent - rat
DOSE/DURATION :
13500 mg/kg/90D-C
TOXIC EFFECTS :
Blood - changes in serum composition (e.g. TP, bilirubin, cholesterol) Blood - changes in erythrocyte (RBC) count Biochemical - Enzyme inhibition, induction, or change in blood or tissue levels - transaminases

MUTATION DATA

TYPE OF TEST :
Mutation in microorganisms
TEST SYSTEM :
Bacteria - Salmonella typhimurium
DOSE/DURATION :
150 ug/plate
REFERENCE :
ESKHA5 Eisei Shikenjo Hokoku. Bulletin of the Institute of Hygienic Sciences. (Kokuritsu Eisei Shikenjo Kagaku, 18-1 Bushitsu Johobu, Setagaya-ku, Tokyo 158, Japan) V.1- 1886- Volume(issue)/page/year: (94),28,1976 *** NIOSH STANDARDS DEVELOPMENT AND SURVEILLANCE DATA *** NIOSH OCCUPATIONAL EXPOSURE SURVEY DATA : NOHS - National Occupational Hazard Survey (1974) NOHS Hazard Code - 83649 No. of Facilities: 211 (estimated) No. of Industries: 4 No. of Occupations: 20 No. of Employees: 7379 (estimated) NOES - National Occupational Exposure Survey (1983) NOES Hazard Code - 83649 No. of Facilities: 63 (estimated) No. of Industries: 4 No. of Occupations: 11 No. of Employees: 4356 (estimated) No. of Female Employees: 530 (estimated)

Safety Information

[ Symbol ]:

GHS07, GHS09

[ Signal Word ]:
Warning

[ Hazard Statements ]:
H302-H317-H319-H410

[ Precautionary Statements ]:
P273-P280-P305 + P351 + P338-P501

[ Personal Protective Equipment ]:
dust mask type N95 (US);Eyeshields;Faceshields;Gloves

[ Hazard Codes ]:
Xn:Harmful;

[ Risk Phrases ]:
R20/22;R36/37/38;R42/43

[ Safety Phrases ]:
S26-S36-S45-S36/37/39

[ RIDADR ]:
UN3077

[ WGK Germany ]:
3

[ RTECS ]:
ST3150000

[ Packaging Group ]:
III

[ Hazard Class ]:
9

[ HS Code ]:
29215990

Synthetic Route

Precursor & DownStream

Customs

[ HS Code ]: 2921590090

[ Summary ]:
2921590090. other aromatic polyamines and their derivatives; salts thereof. VAT:17.0%. Tax rebate rate:13.0%. . MFN tariff:6.5%. General tariff:30.0%

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