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3-二甲氨基苯丙酮盐酸盐

3-二甲氨基苯丙酮盐酸盐用途

【用途一】
用于有机合成。

3-二甲氨基苯丙酮盐酸盐名称

[ CAS 号 ]:
879-72-1

[ 中文名 ]:
β-(二甲氨基)苯丙酮盐酸盐

[ 英文名 ]:
3-DIMETHYLAMINOPROPIOPHENONE HYDROCHLORIDE

[中文别名 ]:

[英文别名 ]:

MFCD00012481
EINECS 212-909-1

3-二甲氨基苯丙酮盐酸盐物理化学性质

[ 沸点 ]:
267.5ºC at 760 mmHg

[ 熔点 ]:
150-155 °C(lit.)

[ 分子式 ]:
C₁₁H₁₆ClNO

[ 分子量 ]:
213.70400

[ 闪点 ]:
91.6ºC

[ 精确质量 ]:
213.09200

[ PSA ]:
20.31000

[ LogP ]:
2.62300

[ 储存条件 ]:
室温

3-二甲氨基苯丙酮盐酸盐MSDS

详细MSDS(安全技术说明书)

3-二甲氨基苯丙酮盐酸盐毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: UH0600000

CHEMICAL NAME :: Propiophenone, 3-(dimethylamino)-, hydrochloride

CAS REGISTRY NUMBER :: 879-72-1

LAST UPDATED :: 199701

DATA ITEMS CITED :: 5

MOLECULAR FORMULA :: C11-H15-N-O.Cl-H

MOLECULAR WEIGHT :: 213.73

WISWESSER LINE NOTATION :: 1N1&2VR &GH

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LDLo - Lowest published lethal dose

ROUTE OF EXPOSURE :: Subcutaneous

SPECIES OBSERVED :: Rodent - rat

DOSE/DURATION :: 200 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: FATOAO Farmakologiya i Toksikologiya (Moscow). For English translation, see PHTXA6 and RPTOAN. (V/O Mezhdunarodnaya Kniga, 113095 Moscow, USSR) V.2- 1939- Volume(issue)/page/year: 25,437,1962

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Oral

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 100 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: AITEAT Archivum Immunologiae et Therapiae Experimentalis. (Ars Polona, POB 1001, 00-068 Warsaw 1, Poland) V.10- 1962- Volume(issue)/page/year: 15,249,1967

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Intraperitoneal

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 70 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: AITEAT Archivum Immunologiae et Therapiae Experimentalis. (Ars Polona, POB 1001, 00-068 Warsaw 1, Poland) V.10- 1962- Volume(issue)/page/year: 15,249,1967

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Subcutaneous

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 223 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: PCJOAU Pharmaceutical Chemistry Journal (English Translation). Translation of KHFZAN. (Plenum Pub. Corp., 233 Spring St., New York, NY 10013) No.1- 1967- Volume(issue)/page/year: 24,833,1990

3-二甲氨基苯丙酮盐酸盐安全信息

[ 符号 ]:

GHS06

[ 信号词 ]:
Danger

[ 危害声明 ]:
H301-H315-H319

[ 警示性声明 ]:
P301 + P310-P305 + P351 + P338

[ 个人防护装备 ]:
Eyeshields;Faceshields;Gloves;type P2 (EN 143) respirator cartridges

[ 危害码 (欧洲) ]:
T: Toxic;

[ 风险声明 (欧洲) ]:
25-36/38

[ 安全声明 (欧洲) ]:
S26-S36/37/39-S45

[ 危险品运输编码 ]:
UN 2811 6.1/PG 3

[ WGK德国 ]:
3

[ RTECS号 ]:
UH0600000

[ 包装等级 ]:
II

[ 危险类别 ]:
6.1

3-二甲氨基苯丙酮盐酸盐合成路线

详细合成路线

3-二甲氨基苯丙酮盐酸盐上下游产品

3-二甲氨基苯丙酮盐酸盐上游产品

3-二甲氨基苯丙酮盐酸盐下游产品

3-二甲氨基苯丙酮盐酸盐制备

将苯乙酮、二甲胺盐酸盐、多聚甲醛、浓盐酸和乙醇配成的混合物加热，回流2h。用丙酮稀释反应物，冷却过夜，滤出粗品。粗品甲乙醇和丙酮重结晶，即得N,N-二甲基-2-苯甲酰乙胺盐酸盐。