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2,4-二硝基二苯胺

2,4-二硝基二苯胺用途

【用途一】
有机合成中间体。

2,4-二硝基二苯胺名称

[ CAS 号 ]:
961-68-2

[ 中文名 ]:
2,4-二硝基二苯胺

[ 英文名 ]:
2,4-Dinitrodiphenylamine

[中文别名 ]:

[英文别名 ]:

2,4-DINITRO-N-PHENYLBENZENAMINE
2,4-Dinitro-N-phenylaniline
2,4-Dinitrodiphenylamine
Benzenamine, 2,4-dinitro-N-phenyl-
N1-phenyl-2,4-dinitroaniline
MFCD00007223
EINECS 213-508-4

2,4-二硝基二苯胺物理化学性质

[ 密度 ]:
1.4±0.1 g/cm3

[ 沸点 ]:
413.8±35.0 °C at 760 mmHg

[ 熔点 ]:
159-161 °C(lit.)

[ 分子式 ]:
C₁₂H₉N₃O₄

[ 分子量 ]:
259.218

[ 闪点 ]:
204.1±25.9 °C

[ 精确质量 ]:
259.059296

[ PSA ]:
103.67000

[ LogP ]:
4.11

[ 外观性状 ]:
红色-棕色粉末

[ 蒸汽压 ]:
0.0±1.0 mmHg at 25°C

[ 折射率 ]:
1.693

[ 储存条件 ]:
库房通风低温干燥,与氧化剂、食品添加剂、酸类分开存放

[ 稳定性 ]:
Stable. Incompatible with strong bases, strong acids, strong oxidizing agents.

2,4-二硝基二苯胺MSDS

2,4-二硝基二苯胺毒性和生态

CHEMICAL IDENTIFICATION

RTECS NUMBER :: JJ8825000

CHEMICAL NAME :: Diphenylamine, 2,4-dinitro-

CAS REGISTRY NUMBER :: 961-68-2

BEILSTEIN REFERENCE NO. :: 1996954

LAST UPDATED :: 199701

DATA ITEMS CITED :: 2

MOLECULAR FORMULA :: C12-H9-N3-O4

MOLECULAR WEIGHT :: 259.24

WISWESSER LINE NOTATION :: WNR CNW DMR

HEALTH HAZARD DATA

ACUTE TOXICITY DATA

TYPE OF TEST :: LD50 - Lethal dose, 50 percent kill

ROUTE OF EXPOSURE :: Intravenous

SPECIES OBSERVED :: Rodent - mouse

DOSE/DURATION :: 180 mg/kg

TOXIC EFFECTS :: Details of toxic effects not reported other than lethal dose value

REFERENCE :: CSLNX* U.S. Army Armament Research & Development Command, Chemical Systems Laboratory, NIOSH Exchange Chemicals. (Aberdeen Proving Ground, MD 21010) Volume(issue)/page/year: NX#06394

2,4-二硝基二苯胺安全信息

[ 符号 ]:

GHS07

[ 信号词 ]:
Warning

[ 危害声明 ]:
H315-H319-H335

[ 警示性声明 ]:
P261-P305 + P351 + P338

[ 个人防护装备 ]:
dust mask type N95 (US);Eyeshields;Gloves

[ 危害码 (欧洲) ]:
Xi:Irritant;

[ 风险声明 (欧洲) ]:
R36/37/38

[ 安全声明 (欧洲) ]:
S26-S37/39

[ 危险品运输编码 ]:
NONH for all modes of transport

[ WGK德国 ]:
3

[ RTECS号 ]:
JJ8825000

[ 海关编码 ]:
2921440000

2,4-二硝基二苯胺合成路线

2,4-二硝基二苯胺上下游产品

2,4-二硝基二苯胺上游产品

2,4-二硝基二苯胺下游产品

2,4-二硝基二苯胺制备

2,4-二硝基氯苯和苯胺按等摩尔比加入水中，先在60℃搅拌反应2h，再在90℃搅拌反应2h。冷却，过滤，洗涤，干燥，得2,4-二硝基二苯胺，收率95-98%。

2,4-二硝基二苯胺海关

[ 海关编码 ]: 2921440000

[ 中文概述 ]:
2921440000. 二苯胺及其衍生物以及它们的盐. 增值税率:17.0%. 退税率:17.0%. 监管条件:无. 最惠国关税:6.5%. 普通关税:30.0%

[ 申报要素 ]: 品名, 成分含量, 用途

[ Summary ]:
2921440000. diphenylamine and its derivatives; salts thereof. VAT:17.0%. Tax rebate rate:17.0%. . MFN tariff:6.5%. General tariff:30.0%

2,4-二硝基二苯胺文献

A novel method for the identification of inorganic and organic gunshot residue particles of lead-free ammunitions from the hands of shooters using scanning laser ablation-ICPMS and Raman micro-spectroscopy.

Analyst 139(23) , 6232-41, (2014)

A method based on scanning laser ablation and inductively coupled plasma-mass spectrometry (SLA-ICPMS) and Raman micro-spectroscopy for the detection and identification of compounds consistent with gu...

Reduction of Nitrated Diphenylamine Derivatives under Anaerobic Conditions.

Appl. Environ. Microbiol. 61(9) , 3282-7, (1995)

2-Nitrodiphenylamine, 4-nitrodiphenylamine, and 2,4-dinitrodiphenylamine were anaerobically metabolized in sediment-water batch enrichments inoculated with mud from the German North Sea coast. The fir...

A simple and efficient anionic chromogenic chemosensor based on 2,4-dinitrodiphenylamine in dimethyl sulfoxide and in dimethyl sulfoxide-water mixtures.

Spectrochim. Acta. A. Mol. Biomol. Spectrosc. 75(2) , 799-806, (2010)

Solutions of 2,4-dinitrodiphenylamine (1) in dimethylsulfoxide (DMSO) are colorless but upon deprotonation they become red. Addition of various anionic species (HSO(4)(-), H(2)PO(4)(-), NO(3)(-), CN(-...

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